Archives for Chemistry Experiments of 5394-13-8

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Single-Electron Transmetalation: Photoredox/Nickel Dual Catalytic Cross-Coupling of Secondary Alkyl beta-Trifluoroboratoketones and -esters with Aryl Bromides

The first cross-coupling of secondary alkyl beta-trifluoroboratoketones and -esters has been achieved through application of photoredox/nickel dual catalysis. Although the related beta-trifluoroboratoamides have been effectively cross-coupled via Pd-catalysis, the corresponding ketones and esters had proven recalcitrant prior to this report. Reactions occur under mild conditions, and a variety of functional groups and sterically and electronically diverse reaction partners are tolerated.

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Reference：
Benzothiophene – Wikipedia,
Benzothiophene | C8H6S – PubChem