6314-28-9, Benzo[b]thiophene-2-carboxylic acid is a benzothiophene compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
6314-28-9, benzo[b]thiophene-2-carboxylic acid (159 mg, 0.892 mmol), 2-amino-biphenyl (156 mg, 0.922 mmol),DCC (393 mg, 1.90mmol)and DMAP (26 mg, 0.21 mmol)was dissolved in dichloromethane (20 mL) and stirred for 14 hours at room temperature. Thin film chromatography (TLC) in verifying, new the spot location changes accordingly once created, after adding water to the composition, a reaction mixture of a, die chloro methane at extracted times 2. Extracted organic layer are dried, in the form of tetrabutylammonium magnesium, was, concentrating it under reduced pressure. Concentrated reaction mixture column chromatography (silica gel, ethyl acetate/n = 1/9-hexanediol) for purifying the white solid thereby, a desired compound (102 mg, 35%) is obtained.
As the paragraph descriping shows that 6314-28-9 is playing an increasingly important role.
Reference£º
Patent; Korea research Institute of Chemical Technology; Han, Soo Bong; Achari, Ragavendra; Kim, Mi Hyeon; Jong, Yong Sik; Kim, Pil Ho; (119 pag.)KR2016/21163; (2016); A;,
Benzothiophene – Wikipedia
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