5381-20-4, Thianaphthene-3-carboxaldehyde is a benzothiophene compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
General procedure: To a flask containing 4.1mmol of a selected aromatic aldehyde in 10.2mL of methanol at 0C were added 0.7452g (5.4mmol) of tyramine. The solution was allowed to stir for 45min and 0.1808g (4.8mmol) of sodium borohydride was added. The solution was allowed to stir for 4.5h, at which point 0.1679g (4.4mmol) of additional sodium borohydride was added. This mixture was stirred overnight and the formed precipitate was collected via vacuum filtration. No further purification was required at this stage. The NMR spectral data for known compounds (2a [51], 2b [50], and 2e [50]) matched those in the literature. The characterization of all new compounds is given below., 5381-20-4
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Reference£º
Article; Henry, Sean; Kidner, Ria; Reisenauer, Mary R.; Magedov, Igor V.; Kiss, Robert; Mathieu, Veronique; Lefranc, Florence; Dasari, Ramesh; Evidente, Antonio; Yu, Xiaojie; Ma, Xiuye; Pertsemlidis, Alexander; Cencic, Regina; Pelletier, Jerry; Cavazos, David A.; Brenner, Andrew J.; Aksenov, Alexander V.; Rogelj, Snezna; Kornienko, Alexander; Frolova, Liliya V.; European Journal of Medicinal Chemistry; vol. 120; (2016); p. 313 – 328;,
Benzothiophene – Wikipedia
Benzothiophene | C8H6S – PubChem