95-15-8, Thianaphthene is a benzothiophene compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
To a CH2Cl2 solution (50 mL) of benzo[b]thiophene (14, 5.00 g, 37.3 mmol) and KOAc (7.30 g, 74.6 mmol) was added Br2 (3.8 mL, 74.6 mmol) at 20 C, and the solution was heated under reflux for 24 h. To the solution was added a satd solution of Na2S2O3 and NaHCO3. The organic and the aqueous layer were separated, and the latter was extracted with CH2Cl2 (3*30 mL). The combined organic layers were dried (Na2SO4), filtered, and concentrated in vacuo. The residue was purified by flash silica column chromatography (pure heptanes) to yield 15a as a white solid (9.1 g, 84%). The spectroscopic data were identical with those reported.
95-15-8 Thianaphthene 7221, abenzothiophene compound, is more and more widely used in various.
Reference£º
Article; Tengho Toguem, Serge-Mitherand; Malik, Imran; Hussain, Munawar; Iqbal, Jamshed; Villinger, Alexander; Langer, Peter; Tetrahedron; vol. 69; 1; (2013); p. 160 – 173;,
Benzothiophene – Wikipedia
Benzothiophene | C8H6S – PubChem