22720-75-8, 2-Acetylbenzothiophene is a benzothiophene compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
To a solution of compound 1 (1.76 g, 12 mmol) and compound 2 (1.76 g, 10 mmol) dissolved in ethanol (20 ml) was added an aqueous solution of potassium hydroxide (1.12 g, 20 mmol) (1.1 ml). The mixture was stirred at room temperature overnight, and water was added to the mixture and precipitates were collected by filtration. The precipitates were washed with water, dissolved in ethyl acetate-THF, and dried over anhydrous magnesium sulfate. Activated charcoal was added to the extract, and the mixture was filtered and the filtrate was concentrated. The residue was triturated from ethyl acetate-isopropyl ether to give compound 3 (2.36 g, 77percent). MS.bul.APCI (m/z): 305/307 ([M+H]+), 22720-75-8
The synthetic route of 22720-75-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Tanabe Seiyaku Co, Ltd.; US2006/135597; (2006); A1;,
Benzothiophene – Wikipedia
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