360576-01-8, Methyl 6-bromobenzo[b]thiophene-2-carboxylate is a benzothiophene compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
A mixture of 900 mg of methyl 6-bromobenzo[b]thiophene-2-caboxylate, 2.28 ml of diisopropylamine, 116 mgof dichlorobis(triphenylphosphine)palladium (II), 32 mg of copper iodide (I), 0.92 ml of trimethylsilyl acetylene, and 15ml of toluene was stirred for 20 hours at room temperature under a nitrogen atmosphere. The filtrate was concentratedunder reduced pressure, the residues were subjected to silica gel column chromatography, thereby obtaining 590 mgof methyl 6-(trimethylsilylethynyl)benzo[b]thiophene-2-carboxylate
The synthetic route of 360576-01-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Sumitomo Chemical Company Limited; MUKUMOTO, Fujio; TAMAKI, Hiroaki; KUSAKA, Shintaro; IWAKOSHI, Mitsuhiko; EP2926660; (2015); A1;,
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